Geochemical characteristics of major and trace elements in Sahinali Coals,Aydin, Turkey

In this study, geochemical behavior of elements is investigated in 25 coal samples collected at 10 locations of ?ahinli coaliferous units at southeast of Ayd?n, Turkey. In all the samples, X-ray powder diffraction and inductively coupled plasma mass spectrometry analyses were performed and element and mineral compositions were determined. Total organic carbon (TOC) values of coals are between 14.6 and 37.7 wt% with average of 28.5 wt%. Samples are composed of quartz, calcite, feldspar, dolomite, mica, gypsum, and salt minerals which are accompanied by illite-, kaolinite-, and smectite-type clay minerals. Comparison of average element contents of world coals and studied samples yields that K > Fe > As > U > Cs > Y > Er > Al > Th > Rb > Yb > W > Tb > Dy > Lu > Ce > Sm > La > Ho > Si > Nd > Gd > Tm > Eu > Nb > Pr > Pb > Sn > Ni > Cu > Ga > Ta > Sb > Zr > Cd > V > Zn > Co > Mo > P > Hf > Ba are found to be enriched, while Mn > Be > Ca > Sr > Bi > Mg are found to be depleted. Statistically elements are correlated with TOC.     

Adsorption Equilibrium Parameters of Trace Impurities

Abstract

Atmospheric air contains various trace impurities which include oxides of nitrogen, carbon, sulphur, and light hydrocarbons. Prior to cryogenic distillation of air to produce oxygen, nitrogen, and argon, these trace impurities have to be removed since many of these compounds constitute a safety hazard in the plant. In this study, adsorption has been considered for their removal and adsorption behavior of ethylene, acetylene, nitrous oxide, acetonitrile, methyl tert-butyl ether, methyl sulfoxide, dimethyl sulfoxide, and methanol have been studied in the Henry's Law low concentration region with several different adsorbents. Adsorption equilibrium parameters have been determined with samples of Alcan pure alumina, Alcan alumina/13X composites Actiguard 600/650PC, CABSORB Chabazite, Ceca13X, and Clinoptilolite by using the concentration pulse chromatographic technique. Heat of adsorption values and van't Hoff plots have been presented.     

高温石墨炉法测定痕量金属的条件选择

高温石墨炉法测定痕量金属对工作条件的要求非常严格,影响分析准确度和精密度的原因较多。从干燥温度和时间,灰化温度和时间,原子化温度和时间,高温除残温度和时间的选择,自动进样器的调整,试样处理等几个方面,合理、正确地选择工作条件能够得到最佳吸收灵敏度和测量精密度。     

基于存储资源迭代重用的低成本寄存器重命名方法

针对超标量深流水线中物理寄存器资源冲突造成的流水线阻塞问题,提出了一种多指令共享同一物理寄存器资源的非阻塞指令发射方法。该方法可在物理寄存器资源冲突下继续分配物理寄存器,利用发射缓冲队列临时缓冲冲突的指令,增加发射流水级实际可分配的物理寄存器数量,释放发射窗口,提高物理寄存器使用的并行性。实验结果表明:相对于传统重命名方法,该方法可减少27.3%的物理寄存器资源实现传统方法相同的性能。     

Quantifying police officers' arrest and self-defence skills: Does performance decrease under pressure?

This study investigated police officers' performance on five selected arrest and self-defence skills that are regularly used in the line of duty. In Experiment 1 a 5-point scale to measure skill performance was developed and tested with 14 police instructors. Results showed that the new scale has satisfactory inter-rater reliability and good intra-rater reliability. In Experiment 2, the external and concurrent validity of the scale was tested by measuring the performances of 19 police officers executing the same skills in a high- and a low-pressure environment and comparing the results obtained with the new 5-point scale with results obtained with a currently used binary scale (i.e. sufficient/insufficient). While the scale proved to have good external and concurrent validity, it appeared that the police officers' performance really suffered under pressure. Given the criticality of successful police performance, it is suggested that incorporating psychological factors (e.g. pressure) in training procedures may enhance performance.     

乙二胺四乙酸四钠中杂质铁的测定

对乙二胺四乙酸四钠中的铁测定,目前主要有两种方法：火焰原子吸收分光光度法和1,10-菲罗琳法。绝大多数用户都采用简便易测的火焰原子吸收分光光度法,但此种方法在不扣除背景的情况下测定结果会因仪器而异。文章通过两台不同型号原子吸收分光光度仪（美国PE-AA100和上海HP-3510）的实验对比表明,在PE-AA100中铁的测定中存在背景吸收,需校正背景,而HP-3510无背景吸收,可直接检测出准确数据。     

夏县地震台痕量氢气突升异常成因的调查与分析

针对2016年9月~10月山西夏县地震台痕量氢气出现的3次大幅突升变化,按照异常核实的时间相关性、空间相关性、强度相关性和机理相关性原则,对异常进行调查分析、实验,结果表明,山西夏县台痕量氢气大幅度变化系交流电源受干扰导致,非震兆异常,提出观测系统整改意见,以期为地震预测提供可靠的观测资料。     

一种基于通讯痕迹的社会网络团伙分析模型

研究在已知目标团伙中某节点以及目标团伙特征的前提下,基于通讯痕迹特征寻找社会网络团伙。研究过程中引入了社会圈、节点中心度和事件集合关联矩阵等概念,重点将聚类分析方法与社会团伙发现相结合,以期得到一种基于通讯痕迹的社会网络团伙分析模型。     

大红袍花椒中微量元素的分析测定

采用4∶1的硝酸和高氯酸的混酸体系作为消化液进行样品消解,火焰原子吸收分光光度法(AAS)测定了陕西韩城大红袍花椒中四种微量元素的含量。结果表明,大红袍花椒中Fe,Mn含量丰富,Zn,Cu含量较少。     

内球面与向心柱面相贯圆角的数控加工研究

针对内球面与向心柱面相贯圆角这一空间曲面,深入研究数控铣削加工该圆角的刀具选择和编程轨迹规划。